反应条件
in benzene-d6 byproducts: H2; under Ar, standard vac. line techniques, in NMR tube; mixt. of (Me3CCH2)P(i-Pr)2, In(CH2CMe3)2Cl and K-In compd. (molar ratio 1:1:1) degassed at-196°C in vac.; benzene-d6 added by vac. dictn.; sealed under va c.; warmed to room temp.; 1 d; not isolated; detd. by (1)H and (31)P NMR spectroscopy;
参考文献
Beachley Jr.; Chao, Sun-Hua L.; Churchill, Melvyn Rowen; Lake, Charles H.
Organometallics, 2001 , vol. 20, # 23 p. 4896 - 4902