in neat (no solvent) mixt. heated (600°C, 12 h) in evacuated silica ampule; homogenized in rocking furnace; quenched in air; annealed near glass transition temp.; XRD;
参考文献
Banser, Deike; Schnell, Melanie; Grabow, Jens-Uwe; Cocinero, Emilio J.; Lesarri, Alberto; Alonso, Jose L.
Angewandte Chemie - International Edition, 2005 , vol. 44, # 39 p. 6311 - 6315
