反应条件
Stage #1: <b>With</b> <a href="#" onclick="return RXDsubstances(event, this, '906771', constants.ctx, '0')">sodium nitrite</a> <b>in</b> <a href="#" onclick="return RXDsubstances(event, this, '3587155', constants.ctx, '0')">water</a>; <a href="#" onclick="return RXDsubstances(event, this, '506007', constants.ctx, '0')">acetic acid</a> <br />T=0°C; 1 h; Inert atmosphereSchlenk technique; <br />Stage #2: <b>With</b> <a href="#" onclick="return RXDsubstances(event, this, '1209320', constants.ctx, '0')">sodium azide</a> <b>in</b> <a href="#" onclick="return RXDsubstances(event, this, '3587155', constants.ctx, '0')">water</a>; <a href="#" onclick="return RXDsubstances(event, this, '506007', constants.ctx, '0')">acetic acid</a> <br />T=0 - 20°C; 1 h; Inert atmosphereSchlenk technique; <br />
参考文献
Alt, Isabel T.; Plietker, Bernd Angewandte Chemie - International Edition, 2016 , vol. 55, # 4 p. 1519 - 1522 Angew. Chem., 2016 , vol. 128, # 4 p. 1542 - 1545,4
