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乙二醇
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63148-62-9
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二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
1207-95-0
合成路线
（共 107 条）
108-86-1
溴代苯
→
反应条件
1207-95-0
反应条件
palladium diacetate; caesium carbonate; tri-cyclo-hexyl-phosphine in o-xylene T=110°C; 8 h;
参考文献
Biro, A. Beatrix; Kotschy, Andras
European Journal of Organic Chemistry, 2007 , # 8 p. 1364 - 1368
1191415-24-3
+
873-55-2
苯亚磺酸钠
→
反应条件
1207-95-0
反应条件
1: 2-(2,2-dibromovinyl)benzenethiol With tetrabutyl ammonium fluoride in N,N-dimethyl-formamide T=20°C; 4 h; Sealed tubeInert atmosphere; 2: benzenesulphinic acid sodium salt With copper diacetate; triethylamine; palladium dichloride in N,N-dimethyl-formamide T=110°C; 12 h; Sealed tubeInert atmosphere;
参考文献
Chen, Wei; Li, Pinhua; Miao, Tao; Meng, Ling-Guo; Wang, Lei
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 3 p. 420 - 424
64345-69-3
→
反应条件
1207-95-0
反应条件
K2S; copper diacetate in N,N-dimethyl-formamide T=140°C; 24 h; Schlenk techniqueInert atmosphere; Reagent/catalyst;
参考文献
Zhang, Xiaoyun; Zeng, Weilan; Yang, Yuan; Huang, Hui; Liang, Yun
Synlett, 2013 , vol. 24, # 13 art. no. ST-2013-W0339-L, p. 1687 - 1692
→
反应条件
1207-95-0
反应条件
[NiCl2(PMe3)2] in tetrahydrofuran T=70°C; 12 h; Inert atmosphere;
参考文献
Liu, Ning; Wang, Zhong-Xia
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 9 p. 1641 - 1645
78602-28-5
→
反应条件
1207-95-0
反应条件
K2S; copper diacetate in N,N-dimethyl-formamide T=140°C; 24 h; Schlenk techniqueInert atmosphere;
参考文献
Zhang, Xiaoyun; Zeng, Weilan; Yang, Yuan; Huang, Hui; Liang, Yun
Synlett, 2013 , vol. 24, # 13 art. no. ST-2013-W0339-L, p. 1687 - 1692
98-91-9
硫代苯甲酸
+
62680-65-3
→
反应条件
1207-95-0
反应条件
tri(n-propyl)amine; copper(l) iodide; 1,10-phenanthroline in 1,4-dioxane T=20 - 100°C; Wittig Olefination; 32.0833 h; Inert atmosphere; Reagent/catalystSolvent;
参考文献
Yu, Hui; Zhang, Meishu; Li, Yuzhe
Journal of Organic Chemistry, 2013 , vol. 78, # 17 p. 8898 - 8903
591-50-4
碘苯
+
95-15-8
苯并噻吩
→
反应条件
63724-94-7
+
1207-95-0
反应条件
copper(l) iodide; 1,10-phenanthroline; tert-BuOD; lithium tert-butylate in N,N'-dimethyl-N,N'-propyleneurea T=125°C; 1 h; Inert atmosphere;
参考文献
Do, Hien-Quang; Khan, Rana M. Kashif; Daugulis, Olafs
Journal of the American Chemical Society, 2008 , vol. 130, # 45 p. 15185 - 15192
92106-62-2
→
反应条件
1207-95-0
反应条件
K2S; copper diacetate in N,N-dimethyl-formamide T=140°C; 24 h; Schlenk techniqueInert atmosphere;
参考文献
Zhang, Xiaoyun; Zeng, Weilan; Yang, Yuan; Huang, Hui; Liang, Yun
Synlett, 2013 , vol. 24, # 13 art. no. ST-2013-W0339-L, p. 1687 - 1692
1191415-24-3
+
2996-92-1
苯基三甲氧基硅烷
→
反应条件
1207-95-0
反应条件
tetrabutyl ammonium fluoride; palladium diacetate; triphenylphosphine in 1-methyl-pyrrolidin-2-one T=80°C; tandem elimination-addition-Hiyama coupling; 12 h;
参考文献
Liu, Jie; Chen, Wei; Ji, Yong; Wang, Lei
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 8 p. 1585 - 1592
1087352-10-0
→
反应条件
1207-95-0
反应条件
oxygen; palladium diacetate; sodium carbonate in cyclohexane T=130°C; 48 h; Molecular sieveSchlenk technique;
参考文献
Modak, Atanu; Naveen, Togati; Maiti, Debabrata
Chemical Communications, 2013 , vol. 49, # 3 p. 252 - 254
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