6-(1’-叔丁基二甲基硅氧乙基)-2-(2’’-四氢呋喃基)培南-3-羧酸烯丙酯合成路线 (共 5 条)
反应条件
triethyl phosphite in xylene 11 h; Heating;
参考文献
Bioorganic and Medicinal Chemistry, , vol. 5, # 7 p. 1389 - 1399
反应条件
1: Et3N / CH2Cl2 / 0.17 h / -20 °C 2: triethyl phosphite / xylene / 11 h / Heating View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 5, # 7 p. 1389 - 1399
反应条件
1: aq. NaHCO3 / acetone / 4 h / 60 °C 2: Et3N / CH2Cl2 / 0.17 h / -20 °C 3: triethyl phosphite / xylene / 11 h / Heating View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 5, # 7 p. 1389 - 1399
反应条件
1: Et3N / CH2Cl2 / 0.17 h / -20 °C 2: triethyl phosphite / xylene / 11 h / Heating View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 5, # 7 p. 1389 - 1399
反应条件
1: AcOH, tetra-n-butylammonium fluoride / tetrahydrofuran / 8.5 h / 50 °C 2: Ph3P, tetrakis(triphenylphosphine)palladium, sodium 2-ethylhexanoate / ethyl acetate / 1 h / Ambient temperature View Scheme
参考文献
Tanaka, Rie; Oyama, Yoshiaki; Imajo, Seiichi; Matsuki, Shinsuke; Ishiguro, Masaji
Bioorganic and Medicinal Chemistry, 1997 , vol. 5, # 7 p. 1389 - 1399