反应条件
1: (3S,4S)-1-methoxy-9-methyl-1-oxo-3-(tetrahydro-2H-pyran-2-yloxy)decan-4-yl benzoate With lithium aluminium tetrahydride in diethyl ether
T=20°C; 0.5 h;
2: methanesulfonyl chloride With triethylamine in diethyl ether
T=0°C;
参考文献
Kovalenko; Masalov; Kulinkovich
Russian Journal of Organic Chemistry, 2009 , vol. 45, # 9 p. 1318 - 1324