4-[(叔-丁基二甲基甲硅烷)氧代]苯甲醛合成路线 （共 42 条）
反应条件
1: 27 percent / NaH / benzene / 16 h / Ambient temperature
2: 80 percent / n-Bu4NF / tetrahydrofuran / 0.5 h / Ambient temperature
3: H2 / 10percent Pd/C / ethyl acetate / 4 h / 2068.6 Torr
View Scheme
参考文献
Cushman, Mark; Nagarathnam, Dhanapalan; Gopal, D.; Chakraborti, Asit K.; Lin, Chii M.; Hamel, Ernest
Journal of Medicinal Chemistry, 1991 , vol. 34, # 8 p. 2579 - 2588
反应条件
1: tetrahydrofuran / 0 °C
2: tetrabutylammonium fluoride / tetrahydrofuran / 20 °C
3: K2CO3 / dimethylformamide / 20 °C
View Scheme
参考文献
Matsuda, Hisashi; Ando, Shin; Morikawa, Toshio; Kataoka, Shinya; Yoshikawa, Masayuki
Bioorganic and Medicinal Chemistry Letters, 2005 , vol. 15, # 7 p. 1949 - 1953
