反应条件
(Z,Z)-1,5-cyclooctadiene in further solvent(s)
Irradiation (UV/VIS); solvent was ethylcyclohexane, reflux under N2 for 18 h; cooled in dry ice/ethanol bath, filtered, recrystd. twice from pentane,sublimation in vac. at 70°C (0.1 mmHg);
参考文献
Moraczewski, Jerome; Geiger, William E.
Journal of the American Chemical Society, 1981 , vol. 103, # 16 p. 4779 - 4787