反应条件
CH3OH; CH3MgI in toluene
byproducts: CO; Sn compd. treated with Fe complex in CS2, then with CH3OH in toluene, Co complex added, heated to 80°C for 1 h, chromd. (Al2O3, CH2Cl2, CH2Cl2/MeOH), evapd. (vac.), stirred for 1 h with CH3MgI in ether at room temp.; hydrolyzed with moist Al2O3 at -80°C, evapd. (vac.), chromd. (Al2O3, pentane), concd., crystd. at -80°C; elem. anal.;
参考文献
Herberich, Gerhard E.; Hessner, Bernd; Beswetherick, Simon; Howard, Judith A.K.; Woodward, Peter
Journal of Organometallic Chemistry, 1980 , vol. 192, # 3 p. 421 - 430
