反应条件
iodine in tetrahydrofuran (N2), I2 added slowly to Co2(CO)8 in THF, stirred at 25°C for 3 h, (C5H4Br)Tl added, stirred for 20 h; filtered, solvent removed in vacuo, mixed with alumina in Et2O, solvent removed, chromd. on alumina with pentane, solvent removed at -40°C/E-3 Torr, contaminated with CpCo(CO)2;
参考文献
Organometallics, , vol. 4, p. 688 - 693
