in n-heptane to soln. of Co complex was added freshly distd. cyclopentadiene at roomtemp. and mixt. was kept for 3 d at room temp.; sepn. of complexes by chromy. (silica gel, hexane); identified by IR;
参考文献
Journal of Organometallic Chemistry, , vol. 188, # 3 p. 373 - 378
in tetrahydrofuran byproducts: fluorenone(1-); Electrolysis; under excess of CO; std. Schlenk and dry-box techniques; at -2.30 V, 0.1 M NBu4PF6, 25°C; not isolated, detected by voltammetry, SSV, coulometry, IR, back electrolys;
参考文献
Inorganica Chimica Acta, , vol. 300-302, p. 96 - 101
in n-heptane byproducts: CO; under Ar, refluxed for 1.5 h; detn. by IR-spectroscopy;
参考文献
Kaganovich, V. S.; Slovokhotov, Yu. L.; Mironov, A. V.; Struchkov, Yu. T.; Rybinskaya, M. I.
Journal of Organometallic Chemistry, 1989 , vol. 372, p. 339 - 350
