3-叔丁基二甲基甲硅烷基-2-丙炔-1-醇合成路线 （共 14 条）
反应条件
sodium bis(2-methoxyethoxy)aluminium dihydride in diethyl ether; toluene 1.5 h; Ambient temperature;
参考文献
Raubo; Wicha
Tetrahedron Asymmetry, 1995 , vol. 6, # 2 p. 577 - 586
反应条件
1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in dimethyl sulfoxide
Inert atmosphere;
参考文献
Mukherjee, Sumit; Kontokosta, Dimitra; Patil, Aditi; Rallapalli, Sivakumar; Lee, Daesung
Journal of Organic Chemistry, 2009 , vol. 74, # 23 p. 9206 - 9209
反应条件
1: Red-Al / diethyl ether; toluene / 1.5 h / cooling
2: 89 percent / mCPBA; Na2HPO4 / CH2Cl2 / 12 h / 20 °C
View Scheme
参考文献
Takeda, Kei; Kawanishi, Eiji; Sasaki, Michiko; Takahashi, Yuji; Yamaguchi, Kentaro
Organic Letters, 2002 , vol. 4, # 9 p. 1511 - 1514
反应条件
1: pyridine / diethyl ether
2: Pd(PPh3)4 / toluene / 1 h / Heating
View Scheme
参考文献
Ogoshi, Sensuke; Nishiguchi, Shinji; Tsutsumi, Ken; Kurosawa, Hideo
Journal of Organic Chemistry, 1995 , vol. 60, # 14 p. 4650 - 4652
