(1,5-环辛二烯)二氯化铂(II)合成路线 （共 69 条）
反应条件
chloroform in chloroform N2-atmosphere; 0.5 h;
参考文献
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), , p. 758 - 760
反应条件
in not given confirmed by microanalysis and NMR spectroscopy data;
参考文献
Organometallics, , vol. 6, p. 788 - 793
反应条件
in chloroform-d1 slight excess of cyclooctadiene was added to a CDCl3 coln. of Pt-complex, reaction was followed by (1)H NMR until equil. was reached; products were identified by their (1)H NMR spectra;
参考文献
Organometallics, , vol. 6, p. 1211 - 1218
反应条件
in chloroform-d1 slight excess of the diolefine was added to a CDCl3 coln. of Pt-complex, reaction was followed by (1)H NMR until equil. was reached; products were identified by their (1)H NMR spectra;
参考文献
Organometallics, , vol. 6, p. 1211 - 1218
反应条件
in chloroform-d1 slight excess of the diolefine was added to a CDCl3 coln. of Pt-complex, reaction was followed by (1)H NMR until equil. was reached; products were identified by their (1)H NMR spectra;
参考文献
Organometallics, , vol. 6, p. 1211 - 1218
反应条件
in chloroform-d1 slight excess of the diolefine was added to a CDCl3 coln. of Pt-complex, reaction was followed by (1)H NMR until equil. was reached; products were identified by their (1)H NMR spectra;
参考文献
Organometallics, , vol. 6, p. 1211 - 1218
反应条件
in hexane byproducts: tri-i-propylphosphine;
参考文献
Journal of the Indian Chemical Society, , vol. 59, # 2 p. 141 - 144
反应条件
in benzene byproducts: tri-t-butylphosphine;
参考文献
Journal of the Indian Chemical Society, , vol. 59, # 2 p. 141 - 144
反应条件
in chloroform N2-atmosphere; equimolar amts. of Pt-complex and PPh3, 1.3 equiv. of Me2NCH2NMe2, standing at room temp. for 4 h; chromy. (silica, TLC, MeOH:CH2Cl2 3:97); NMR-spectroscopy;
参考文献
Organometallics, , vol. 18, # 13 p. 2428 - 2439
反应条件
in dichloromethane room temp., N2 atm.; to a soln. of Pt-complex in CH2Cl2 solid diarsine was added, the mixt. was stirred at room temp. for 3 h; filtered, washed with diethyl ether, vac. dried; elem. anal.;
参考文献
Novio, Fernando; Mas-Balleste, Ruben; Gallardo, Iluminada; Gonzalez-Duarte, Pilar; Lledos, Agusti; Vila, Neus
Dalton Transactions, 2005 , # 16 p. 2742 - 2753
