byproducts: H2; heating of the diborane and the phosphinoylborane to 120°C, stirring for 2 h, cooling to 20°C, all steps under exclusion of air and moisture; monitored by NMR;
heating of the diborane and the phosphinoylborane to 120°C, stirring for 2 h, cooling to 20°C, all steps under exclusion of air and moisture; monitored by NMR;
参考文献
Koester, Roland; Schuessler, Wilhelm; Synoradzki, Ludwik
Chemische Berichte, 1987 , vol. 120, p. 1105 - 1116
