Koester, R.; Grassberger, M. A.
Liebigs Annalen der Chemie, 1968 , vol. 719, p. 169 - 186
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Gmelin Handbook: B: B-Verb.9, 6.3.2, page 303 - 314
decene-1
introduction of BCl3 in mixt. of B(n-C3H7) and (C2H5)2B2H2 for 15 min, addn. of decene-1; distn.;
参考文献
Koester, R.; Grassberger, M. A.
Liebigs Annalen der Chemie, 1968 , vol. 719, p. 169 - 186
Full Text Show Details
Gmelin Handbook: B: B-Verb.9, 6.2.2, page 269 - 280
byproducts: H2, PH3; dropwise addn. of the phosphate to heated and stirred diborane at 80-105°C over 2 h, heating to 110°C at 1,5 h, all steps under air and moisture exclusion; monitored by NMR;
参考文献
Koester, Roland; Schuessler, Wilhelm; Synoradzki, Ludwik
Chemische Berichte, 1987 , vol. 120, p. 1105 - 1116
