(1-氯-2-甲酰基乙烯基)二茂铁合成路线 （共 7 条）
反应条件
NaOH in sodium hydroxide aq. NaOH; Fe complex was treated with 1 N NaOH;
参考文献
Jacques, Beatrice; Tranchier, Jean-Philippe; Rose-Munch, Francoise; Rose, Eric; Stephenson, G. Richard; Guyard-Duhayon, Carine
Organometallics, 2004 , vol. 23, # 2 p. 184 - 193
反应条件
in ethanol 30-40°C;;
参考文献
Schloegl, K.; Steyrer, W.
Monatshefte fuer Chemie, 1965 , vol. 96, p. 1520 - 1535
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Gmelin Handbook: Fe: Org.Verb.A1, 5.1.1.3.1, page 296 - 299
反应条件
NaO2CCH3 in N,N-dimethyl-formamide
acetylferrocene was treated with POCl3, DMF and NaO2CCH3;
参考文献
Jacques, Beatrice; Tranchier, Jean-Philippe; Rose-Munch, Francoise; Rose, Eric; Stephenson, G. Richard; Guyard-Duhayon, Carine
Organometallics, 2004 , vol. 23, # 2 p. 184 - 193
反应条件
sodium carbonate in water; acetone
aq. satd. sodium carbonate soln. added to the Fe-complex in acetone, mixt. stirred for 5 min; water added, mixt. extd. (ether); ether soln. washed (water), dried (Na2SO4), evapn.;
参考文献
Boev, V. I.; Dombrovskii, A. V.
Journal of General Chemistry USSR (English Translation), 1984 , vol. 54, p. 1439 - 1443
Zhurnal Obshchei Khimii, 1984 , vol. 54, p. 1617 - 1622
反应条件
sodium carbonate in water; acetone
aq. satd. sodium carbonate soln. added to the Fe-complex in acetone, mixt. stirred for 5 min; water added, mixt. extd. (ether); ether soln. washed (water), dried (Na2SO4), evapn.;
参考文献
Boev, V. I.; Dombrovskii, A. V.
Journal of General Chemistry USSR (English Translation), 1984 , vol. 54, p. 1439 - 1443
Zhurnal Obshchei Khimii, 1984 , vol. 54, p. 1617 - 1622
反应条件
in N,N-dimethyl-formamide
according to Polin J., et al., Organic Syntheses, 1996, 73, 262;
参考文献
Zora, Metin; Goermen, Meral
Journal of Organometallic Chemistry, 2007 , vol. 692, # 22 p. 5026 - 5032
反应条件
trichlorophosphate
Cooling with ice;
参考文献
Wu, Chao; Liang, Zhi-Wu; Xu, Ying-Ying; He, Wei-Min; Xiang, Jian-Nan
Chinese Chemical Letters, 2013 , vol. 24, # 12 p. 1064 - 1066
