Nesmeyanov, A. N.; Iurieva, L. P.; Levchenko, S. N.
Doklady Akademii Nauk SSSR, 1970 , vol. 190, p. 118 - 121
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Gmelin Handbook: Cr: Org.Verb., 1.6.2.1.4, page 352 - 355
methyl iodide in hexane under ice cooling, hydrolysis, M ratio of (m-CH3C6H4CH3)2Cr, (p-CH3C6H4CH3)2Cr and (2.3.5-(CH3)3C6H3)2Cr=11:13.2:3.8:7.3; chromy.;
methyl iodide in hexane under ice cooling, hydrolysis, M ratio of (m-CH3C6H4CH3)2Cr, (p-CH3C6H4CH3)2Cr and (2.3.5-(CH3)3C6H3)2Cr=11:13.2:3.8:7.3; chromy.;
benzene in benzene
byproducts: methylcyclohexane, toluene, methylcyclohexene; Cr was cocondensed with 4-methylcyclohex-1-ene at liq. N2 temp., the reaction flask was vented with dry and Ar, arene was added;
参考文献
Shepherd, M. C.; Jagannathan, R.; Lagowski, J. J.
Journal of the American Chemical Society, 1984 , vol. 106, p. 7647 - 7649
