triphenylphosphine in benzene
byproducts: Fe(CO)4P(C6H5)3, Fe(CO)3(P(C6H5)3)2; (Ar), mixture was heated at 140°C for 4 h in a sealed tube; GC, (1H)-NMR;
参考文献
Barrau, Jacques; Hamida, Najib Ben; Agrebi, Hamid; Satge, Jacques
Inorganic Chemistry, 1990 , vol. 29, p. 1674 - 1678
With iodine in neat (no solvent) mixt. of (CH3)2Ge(CH2)2Ge(CH3)2Fe(CO)4 and I2 heated (140°C) for 8h at 140°C in a sealed tube under argon; determination: GC and 1H-NMR;
参考文献
Barrau, Jacques; Hamida, Najib Ben; Agrebi, Abdelhamid; Satge, Jacques Organometallics, 1989 , vol. 8, p. 1585 - 1593
With bromine in neat (no solvent) mixt. of (CH3)2Ge(CH2)2Ge(CH3)2Fe(CO)4 and Br2 heated (140°C) for 8h in a sealed tube under argon; determination: GC and 1H-NMR;
参考文献
Barrau, Jacques; Hamida, Najib Ben; Agrebi, Abdelhamid; Satge, Jacques Organometallics, 1989 , vol. 8, p. 1585 - 1593
