反应条件
t-BuOK; n-BuLi in tetrahydrofuran; hexane dropwise addn. of BuLi (2.5 M, hexane, 1 h) to soln. (THF) of Cp-deriv. (-78°C), mixing with soln. (THF) of Fe-intermediate (made from t-BuOK and Fe-compd., 0°C, 30 min), heating (60°C, 6 h); cooling to room temp. extn. (hexane-water (+ HCl drop)), org. phase drying (MgSO4), concg., chromy. (SiO2, hexane);
参考文献
Lee, Si-Geun; Lee, Hee-Kyu; Lee, Su Seong; Chung, Young Keun
Organometallics, 1997 , vol. 16, # 3 p. 304 - 306
