反应条件
in diethyl ether; water all manipulations under inert atm.; AgNO3 dissolved in water, aq. NaOH added in excess, added soln. of Fe complex in Et2O, vigorously stirred atroom temp. for 1.5-2 h; filtered, washed with water, filtrate concd. in vac., cooled, added glacial AcOH, filtered, washed with water, with dild. aq. NH3, repptd. with glacial AcOH or HCl;
参考文献
Neto, Alberto Federman; Miller, Joseph; De Andrade, Vania Faria; Fujimoto, Susana Yumi; De Freitas Afonso, Marcia Maisa; Archanjo, Fernando Costa; Darin, Vitor Andre; Andrade E Silva, Marcio Luis; Borges, Aurea Donizete Lanchote; Del Ponte, Gino
Zeitschrift fur Anorganische und Allgemeine Chemie, 2002 , vol. 628, # 1 p. 209 - 216
