反应条件
sodium hydroxide in solid
thorough grounding a mixt. of aldehyde and phosphonium salt with NaOH atroom temp., heating at 65°C for 240 min, grounding for 1-2 min, cooling to room temp.; extn. with CH2Cl2, drying with Na2SO4, filtration, evapn., chromy (SiO2,petroleum ether);
参考文献
Liu, Wan-Yi; Xu, Qi-Hai; Ma, Yong-Xiang; Liang, Yong-Min; Dong, Ning-Li; Guan, De-Peng
Journal of Organometallic Chemistry, 2001 , vol. 625, # 1 p. 128 - 131
