2-氨基-5-硝基三氟甲苯合成路线 （共 26 条）
反应条件
sodium azide; CuSO4‵5H2O; sodium carbonate; sodium L-ascorbate; L-proline in water; dimethyl sulfoxide T=70°C; 24 h;
参考文献
Tetrahedron, , vol. 66, # 38 p. 7642 - 7650
反应条件
potassium hydroxide; N,N-tetramethylene-thiocarbamoyl-sulphenamide in ammonia
参考文献
Journal of Organic Chemistry, , vol. 57, # 18 p. 4784 - 4785
反应条件
1: With 5-(2-hydroxyethyl)-4-methyl-3-(phenylmethyl)thiazolium chloride; tert-butyl alcohol in tetrahydrofuran T=20°C; 0.0833333 h; Inert atmosphere; 2: With sodium t-butanolate in tetrahydrofuran T=20°C; 12 h; Inert atmosphere; chemoselective reaction;
参考文献
Synlett, , vol. 24, # 5 art. no. ST-2013-D0038-L, p. 652 - 656
反应条件
sodium hydroxide in N-methyl-acetamide; methanol; ammonia; water
反应条件
potassium tert-butylate; N,N-tetramethylene-thiocarbamoyl-sulphenamide in N,N-dimethyl-formamide T=20°C; 0.333333 h;
参考文献
Journal of Organic Chemistry, , vol. 63, # 15 p. 4878 - 4888
反应条件
4-nitro-4-methyl-2,3,5,6-tetrabromo-2,5-cyclohexadien-1-one in trifluoroacetic acid 3 h; Ambient temperature;
参考文献
Synthesis, , # 10 p. 761 - 763
反应条件
methoxylamine hydrochloride; potassium tert-butylate; copper(l) chloride in N,N-dimethyl-formamide 1 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 61, # 2 p. 442 - 443
反应条件
1: HNO3, H2SO4 2: liq. NH3 View Scheme
参考文献
Journal of Organic Chemistry, , vol. 26, p. 2707 - 2710
参考文献
Journal of the Chemical Society, , p. 3459,3463
Journal of the Chemical Society, , p. 1071,1074
反应条件
1: H2SO4; HNO3 2: aq.-ethanolic NaOH View Scheme
参考文献
Journal of the Chemical Society, , p. 3459,3463
Journal of the Chemical Society, , p. 1071,1074
