sodium hydride in dimethyl sulfoxide T=25°C; 17 h; NaH : pyrocatechlol 2.2; Yields of byproduct given;
参考文献
Kessar, Satinder V.; Gupta, Yash P.; Mohammad, Taj; Goyal, Manju; Sawal, Kewal K.
Journal of the Chemical Society, Chemical Communications, 1983 , # 7 p. 400 - 401
1: (+/-)-1-bromo-4-(1-ethoxyethyl)-3-methoxybenzene With n-butyllithium in tetrahydrofuran; hexane T=-78°C; Metallation; 2 h; 2: N,N-dimethyl-formamide in tetrahydrofuran; hexane T=-78 - 20°C; Condensation; 18 h; 3: With hydrogenchloride in water Hydrolysis; 0.5 h;
参考文献
Parveen, Ifat; Threadgill, Michael D.
Journal of Labelled Compounds and Radiopharmaceuticals, 2000 , vol. 43, # 9 p. 883 - 889
