反应条件
n-butyllithium in tetrahydrofuran dissolved aromatic bromide in THF, added n-BuLi dropwise, mixt. stirredat -78°C for 15 min; added freshly distd. (CH3O)3B, stirred at -78°C for 30 min, warmed to room temp., stirred for further 20 min; cooled to 0°C, acidified, extracted with CH2Cl2, dried, evapd. under vac.;
参考文献
De Koning, Charles B.; Michael, Joseph P.; Rousseau, Amanda L.
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 5 p. 787 - 797
