反应条件
n-butyllithium in tetrahydrofuran N2; BuLi dropping into org. compd. soln. at -78°C, mixt. keeping 3 h, B-compd. soln. addn. dropwise at -78°C, mixt. allowing to warm to room temp. overnight , stirring 1 h with 10percent HCl, extn. (Et2O); org. extracts washing (water), drying, solvent vac. removal;
参考文献
Liu, Shu-Juan; Zhao, Qiang; Fan, Qu-Li; Huang, Wei
European Journal of Inorganic Chemistry, 2008 , # 13 p. 2177 - 2185