反应条件
n-butyllithium in diethyl ether; hexane; toluene N2 atmosphere, addn. of n-BuLi in hexane to BrC6H4CH2SEt in ether (-78°C), warming to room temp., addn. of B(OMe)3 in ether (-78°C), warming to room temp., addn. of aq. H2SO4, evapn. of ether phase, addn. of (HOC(CH3)2)2 in toluene (2 h); fractional distn.; elem. anal.;
参考文献
Oki, Michinori; Yamada, Yasuhisa
Bulletin of the Chemical Society of Japan, 1988 , vol. 61, p. 1191 - 1194
