Lappert,M.F. et al.
Journal of the Chemical Society [Section] A: Inorganic, Physical, Theoretical, 1970 , p. 2320 - 2324
Full Text View citing articles Show Details
Gmelin Handbook: B: B-Verb.9, 3.2.10, page 75 - 75
1: 5-bromo-3-methoxytoluene With n-butyllithium in tetrahydrofuran; hexane
T=-78°C; 0.5 h;
2: boric acid trimethyl ester in tetrahydrofuran; hexane
T=-78 - 20°C; 1.5 h;
3: With hydrogenchloride; water
more than 3 stages;
参考文献
SMITHKLINE BEECHAM CORPORATION; VITAE PHARMACEUTICALS, INC.
Patent: WO2008/124575 A1, 2008 ;
Location in patent: Page/Page column 128-139 ;
WO 2008/124575 A1
benzene
byproducts: H2O; dehydration with benzene;;
参考文献
McCusker et al.
Journal of the American Chemical Society, 1957 , vol. 79, p. 5179
View citing articles Show Details
Gmelin Handbook: B: B-Verb.13, 4.7.2.2, page 189 - 196