反应条件
in neat (no solvent) condensing a slight excess of methanol with BCl3 at 75 K, warming to -85°C for about 30 min.; traces of methanol present in the product; fractionating through baths at -90°C and -196°C;
参考文献
McKean, D. C.; Coats, A. M.
Spectrochimica Acta, Part A: Molecular and Biomolecular Spectroscopy, 1989 , vol. 45, # 3 p. 409 - 420
