反应条件
in benzene-d6
inert atmosphere; stirring at room temp. for 1 h, then refluxing for 72 h; cooling, removal of volatiles (vac.), extn. into pentane, filtration, solvent removal (vac.), recrystn. (MeOH/water=1:6, room temp.); elem. anal.;
参考文献
Brain, Paul T.; Cowie, Jill; Donohoe, David J.; Hnyk, Drahomir; Rankin, David W.H.; Reed, David; Reid, Bruce D.; Robertson, Heather E.; Welch, Alan J.; Hofmann, Matthias; Von Schleyer, Paul Rague
Inorganic Chemistry, 1996 , vol. 35, # 6 p. 1701 - 1708