反应条件
1: 2.) air / 1.) THF, room temp., 24 h; 2.) diethyl ether, water, -60 deg C - -50 deg C, 1h. 2: metallic potassium / tetrahydrofuran / 2.5 h / Ambient temperature 3: 1.) N,N,N-trimethylphenylammonium perchlorate; 2.) air / 1.) THF, room temp., 24 h; 2.) diethyl ether, water, -60 deg C - -50 deg C, 1h. View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 18, # 10 p. 1888 - 1896
Zhurnal Organicheskoi Khimii, , vol. 18, # 10 p. 2143 - 2152
