反应条件
1: 1.) NaOH, 2.) HCl / 1.) aq. ethanol, room temperature, 20 h, 2.) water, ethanol, 5 deg C, 5 h 2: NaOH / ethanol 3: 88 percent / NaOH, hydrogen / tris(triphenylphosphine)rhodium(I) chloride / ethanol / 2068.6 Torr / Ambient temperature 4: 88 percent / sulfuric acid / 17 h / Heating 5: 92 percent / triethylamine / CH2Cl2 / 0 °C 6: 66 percent / palladium(II) acetate, triphenylphosphine, lithium bromide, triethylamine / toluene / 6 h / 100 °C / other reagent: tri-o-tolylphosphine View Scheme
参考文献
Larsen, Robert D.; Corley, Edward G.; King, Anthony O.; Carroll, James D.; Davis, Paul; Verhoeven, Thomas R.; Reider, Paul J.; Labelle, Marc; Gauthier, Jacques Y.; Xiang, Yi Bin; Zamboni, Robert J.
Journal of Organic Chemistry, 1996 , vol. 61, # 10 p. 3398 - 3405