甲基4-甲氧基苯甲酸酯合成路线 （共 354 条）
反应条件
methanol; 1,1-dimethylpropan-1-ol; sodium hydride; anhydrous cobalt diacetate in tetrahydrofuran T=40°C; P=760 Torr; 16 h; Irradiation;
参考文献
Journal of Organic Chemistry, , vol. 60, # 26 p. 8336 - 8340
反应条件
tetrabutyl ammonium fluoride; (t-Bu2POH)2PdCl2 in acetonitrile T=50°C; 24 h;
参考文献
Lerebours, Rachel; Wolf, Christian
Journal of the American Chemical Society, 2006 , vol. 128, # 40 p. 13052 - 13053
反应条件
in N,N-dimethyl-formamide T=140°C; 0.5 h; Microwave irradiation;
参考文献
Belov, Pavel; Campanella, Veronica L.; Smith, Alison W.; Priefer, Ronny
Tetrahedron Letters, 2011 , vol. 52, # 21 p. 2776 - 2779
反应条件
in N,N-dimethyl-formamide T=140°C; 0.5 h; Microwave irradiation;
参考文献
Belov, Pavel; Campanella, Veronica L.; Smith, Alison W.; Priefer, Ronny
Tetrahedron Letters, 2011 , vol. 52, # 21 p. 2776 - 2779
反应条件
1: (4-methoxyphenyl)methanol With sodium chlorite; sodium dihydrogenphosphate; 1-MeAZADO(1+)*Cl(1-) in dichloromethane; water T=25°C; 10 h; 2: With 2-methyl-but-2-ene in dichloromethane; water 3: diazomethane With hydrogenchloride; sodium hydroxide Product distribution / selectivity; more than 3 stages;
参考文献
Nissan Chemical Industries, Ltd.
Patent: US2009/124806 A1, 2009 ;
Location in patent: Page/Page column 5-7 ;
反应条件
1: 1-bromo-4-methoxy-benzene With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 0.5 h; 2: N,N-dimethyl-formamide in tetrahydrofuran; hexane T=-78 - 20°C; 2 h; 3: methanol Further stages;
参考文献
Tetrahedron, , vol. 68, # 24 p. 4701 - 4709
反应条件
triethylamine; palladium on activated charcoal T=130°C; Sonogashira coupling; P=3750.38 Torr; 2 h;
参考文献
Mei, Hui; Xiao, Se; Zhu, Tianwu; Lei, Yizhu; Li, Guangxing
Transition Metal Chemistry, 2014 , vol. 39, # 4 p. 443 - 450
反应条件
[RhCl(η2:η2-cycloocta-1,5-diene)]2; tri-n-butyl phosphite; tri-iso-propylsilane in 2-cyclohexylethanol T=130°C; 15 h; Inert atmosphere;
参考文献
Tobisu, Mamoru; Nakamura, Ryo; Kita, Yusuke; Chatani, Naoto
Journal of the American Chemical Society, 2009 , vol. 131, p. 3174 - 3175
反应条件
dcpp*2HBF4; palladium diacetate; potassium carbonate in dimethyl sulfoxide T=120°C; P=760.051 Torr; 15 h; Molecular sieve;
参考文献
Watson, Donald A.; Fan, Xuexiang; Buchwald, Stephen L.
Journal of Organic Chemistry, 2008 , vol. 73, # 18 p. 7096 - 7101
反应条件
CuF2 in water; dimethyl sulfoxide T=120°C; 12 h; Schlenk techniqueInert atmosphereGreen chemistry;
参考文献
Tetrahedron Letters, , vol. 55, # 2 p. 390 - 393
