甲基4-甲氧基苯甲酸酯合成路线 (共 354 条)
反应条件
methyl iodide in toluene T=100 - 115°C; 40 h;
参考文献
Yamamoto, Yasushi; Shimizu, Hideaki; Hamada, Yoshitaka
Journal of Organometallic Chemistry, 1996 , vol. 509, # 2 p. 119 - 122
反应条件
1: hydroxylamine hydrochloride; potassium hydroxide / methanol / 24 h / |Reflux 2: 1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine; 1,8-diazabicyclo[5.4.0]undec-7-ene; 1,4-diaza-bicyclo[2.2.2]octane; triethylamine / methanol / 3 h / |Reflux; |Green chemistry View Scheme
参考文献
Kreye, Oliver; Wald, Sarah; Meier, Michael A. R.
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 1 p. 81 - 86
反应条件
sodium hexamethyldisilazane in tetrahydrofuran T=185°C; 24 h;
参考文献
Synthesis, , # 3 p. 329 - 332
反应条件
sodium hexamethyldisilazane in tetrahydrofuran T=110°C; 24 h;
参考文献
Synthesis, , # 3 p. 329 - 332
反应条件
indium trifluoromethanesulfonate; N-iodo-succinimide in acetonitrile T=23°C; 36 h; Inert atmosphereDarkness;
参考文献
Organic Letters, , vol. 12, # 9 p. 2104 - 2107
反应条件
dimethyl zinc; sodium hydride in tetrahydrofuran T=0°C; 6 h;
参考文献
Uchiyama, Masanobu; Furumoto, Shozo; Saito, Mariko; Kondo, Yoshinori; Sakamoto, Takao
Journal of the American Chemical Society, 1997 , vol. 119, # 47 p. 11425 - 11433
反应条件
1: With [CpFe(CO)2(PCy3)][BF4]; phenyl silane T=100°C; 24 h; IrradiationNeat (no solvent)Inert atmosphere; 2: With hydrogenchloride; water in tetrahydrofuran T=20°C; 1 h;
参考文献
Bezier, David; Venkanna, Gopaladasu T.; Castro, Luis C. Misal; Zheng, Jianxia; Roisnel, Thierry; Sortais, Jean-Baptiste; Darcel, Christophe
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 10 p. 1879 - 1884
反应条件
tetraethylammonium p-toluenesulfonate Electrochemical reactionSn cathode; Pt anode; constant current 0.2 A; divided cell;
参考文献
Journal of Organic Chemistry, , vol. 66, # 3 p. 862 - 867
反应条件
AlBrCl3(1-)*C5H5N*H(1+) T=140°C; 3 h;
参考文献
Wei, Ben-Mei; Zhang, Zhi-Yong; Dai, Zhi-Qun; Zhang, Kai-Cheng
Monatshefte fur Chemie, 2011 , vol. 142, # 10 p. 1029 - 1033
反应条件
aluminium trichloride; lauryl mercaptan T=20°C; 4.5 h;
参考文献
Tetrahedron Letters, , vol. 42, # 52 p. 9207 - 9210
Monatshefte fur Chemie, , vol. 135, # 2 p. 189 - 200