甲基4-甲氧基苯甲酸酯合成路线 (共 354 条)
反应条件
bismuth(III) chloride; palladium diacetate; potassium carbonate T=20°C; 2 h; chemoselective reaction;
参考文献
Bai, Xing-Feng; Ye, Fei; Zheng, Long-Sheng; Lai, Guo-Qiao; Xia, Chun-Gu; Xu, Li-Wen
Chemical Communications, 2012 , vol. 48, # 68 p. 8592 - 8594
反应条件
1: 1-bromo-4-methoxy-benzene With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 0.5 h; 2: N,N-dimethyl-formamide in tetrahydrofuran; hexane T=-78 - 20°C; 2 h; 3: methanol Further stages;
参考文献
Tetrahedron, , vol. 68, # 24 p. 4701 - 4709
反应条件
in toluene T=200°C; 16 h; Inert atmosphere;
参考文献
Lee, Jennifer J.; Kraus, George A.
Tetrahedron Letters, 2013 , vol. 54, # 19 p. 2366 - 2368
反应条件
CoCRACO; sodium tert-pentoxide; sodium hydride in tetrahydrofuran 40 h; Irradiation;
参考文献
Synthetic Communications, , vol. 23, # 10 p. 1361 - 1370
反应条件
potassium hydroxide in tetrahydrofuran; methanol; water T=20°C;
参考文献
Mastronardi, Federica; Gutmann, Bernhard; Oliver Kappe
Organic Letters, 2013 , vol. 15, # 21 p. 5590 - 5593
反应条件
tert.-butylhydroperoxide; sodium hydrogencarbonate; cis-(2,2)-Rh2(cap)4 in decane; 1,2-dichloro-ethane T=40°C; 16 h;
参考文献
Catino, Arthur J.; Nichols, Jason M.; Choi, Hojae; Gottipamula, Sidhartha; Doyle, Michael P.
Organic Letters, 2005 , vol. 7, # 23 p. 5167 - 5170
反应条件
1: methyl 4-hydroxy-benzoate With sodium hydride in N,N-dimethyl-formamide T=0°C; 0.333333 h; 2: methyl iodide in N,N-dimethyl-formamide T=20°C; 15 h;
参考文献
Srensen, Ulrik S.; Falch, Erik; Stensbl, Tine B.; Jaroszewski, Jerzy W.; Madsen, Ulf; Krogsgaard-Larsen, Povl
Archiv der Pharmazie, 2001 , vol. 334, # 2 p. 62 - 68
反应条件
copper(l) chloride in chlorobenzene T=130°C; 12 h; Schlenk techniqueInert atmosphere;
参考文献
Xia, Qinqin; Liu, Xiaolong; Zhang, Yuejiao; Chen, Chao; Chen, Wanzhi
Organic Letters, 2013 , vol. 15, # 13 p. 3326 - 3329
反应条件
in methanol T=20°C; 0.166667 h;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 22, # 12 p. 3993 - 3997
反应条件
5 palladium on charcoal; oxygen in methanol T=60°C; P=760.051 Torr; 1 h;
参考文献
Powell, Adam B.; Stahl, Shannon S.
Organic Letters, 2013 , vol. 15, # 19 p. 5072 - 5075