甲基4-甲氧基苯甲酸酯合成路线 （共 354 条）
反应条件
1: NaH / 1,2-dimethoxy-ethane; paraffin / 4 h / Heating
2: piperidine / ethanol / Heating
View Scheme
参考文献
Specht, Donald P.; Martic, Peter A.; Farid, Samir; ++
Tetrahedron, 1982 , vol. 38, # 9 p. 1203 - 1211
反应条件
in tetrahydrofuran
T=0°C; 0.5 h;
参考文献
Pine, Stanley H.; Pettit, Robert J.; Geib, Gregory D.; Cruz, Susana G.; Gallego, Claudio H.; et al.
Journal of Organic Chemistry, 1985 , vol. 50, # 8 p. 1212 - 1216
反应条件
N(Et)4ClO4 in N,N-dimethyl-formamide
Ambient temperatureelectrolysis;
参考文献
Arai; Tamura; Kawai; Nakajima
Chemical and Pharmaceutical Bulletin, 1989 , vol. 37, # 11 p. 3117 - 3118
反应条件
1: 56 percent / NaH / dimethylsulfoxide; diethyl ether / 12 h / 20 °C
2: pyridine; Br2 / CH2Cl2 / 0.5 h / -5 °C
View Scheme
参考文献
Douadi, Tahar; Cariou, Michel
Phosphorus, Sulfur and Silicon and the Related Elements, 2003 , vol. 178, # 3 p. 509 - 520
反应条件
Triton X-114; thiolacetic acid potassium salt
T=150°C;
参考文献
Bhattacharya, Apurba; Patel, Nitin C.; Vasques, Tomas; Tichkule, Ritesh; Parmar, Gaurang; Wu, Jiejun
Tetrahedron Letters, 2006 , vol. 47, # 4 p. 565 - 567
反应条件
Multi-step reaction with 2 steps 1: ethanol / Heating2: HCl(conc) / methanol / 4 h / Heating
参考文献
Balse, Mukta N.; Mahajanshetti, C. S. Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1980 , vol. 19, # 4 p. 260 - 262
反应条件
Multi-step reaction with 2 steps 1: hydrazine hydrate / methanol / 6 h / |Reflux2: acetic acid / methanol / 3 h / |Reflux
参考文献
Taha, Muhammad; Naz, Humera; Rasheed, Saima; Ismail, Nor Hadiani; Rahman, Aqilah Abd; Yousuf, Sammer; Choudhary, Muhammad Iqbal Molecules, 2014 , vol. 19, # 1 p. 1286 - 1301
反应条件
Multi-step reaction with 2 steps 1: hydrazine hydrate / methanol / 6 h / |Reflux2: acetic acid / methanol / 3 h / |Reflux
参考文献
Taha, Muhammad; Naz, Humera; Rasheed, Saima; Ismail, Nor Hadiani; Rahman, Aqilah Abd; Yousuf, Sammer; Choudhary, Muhammad Iqbal Molecules, 2014 , vol. 19, # 1 p. 1286 - 1301
反应条件
Multi-step reaction with 2 steps 1: 70 percent / 1.) sec-BuLi / 1.) -105 deg C2: 98 percent / formic acid / 1 h / Heating
参考文献
Date, Matsuhiro; Kawanishi, Kenji; Hori, Takako; Watanabe, Mitsuaki; Furukawa, Sunao Chemical & Pharmaceutical Bulletin, 1989 , vol. 37, # 10 p. 2884 - 2886
反应条件
With toluene-4-sulfonic acid in methanol Heating;
参考文献
D'Anello, Matteo; Erba, Emanuela; Gelmi, Maria Luisa; Pocar, Donato Chemische Berichte, 1988 , vol. 121, p. 67 - 74
