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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
9-氰基蒽
合成路线
（共 61 条）
18004-57-4
蒽-9-甲醛肟
→
反应条件
1210-12-4
9-氰基蒽
反应条件
1: With 2-chloro-1-methyl-pyridinium iodide in dichloromethane T=20°C; 0.166667 h; 2: With triethylamine in dichloromethane T=20°C; 2 h;
参考文献
Sardarian; Shahsavari-Fard; Shahsavari; Ebrahimi
Tetrahedron Letters, 2007 , vol. 48, # 14 p. 2639 - 2643
120-12-7
蒽
+
93-61-8
甲基甲酰苯胺
→
反应条件
1210-12-4
9-氰基蒽
反应条件
1: N-methyl-N-formyl-aniline With diphosphoric acid tetrachloride T=0°C; 0.5 h; 2: anthracene in N,N-dimethyl-formamide T=100°C; Vilsmeier-Haack reaction; 10 h; 3: With ammonia; iodine in tetrahydrofuran; water; N,N-dimethyl-formamide T=20°C; 3 h; regioselective reaction;
参考文献
Ushijima, Sousuke; Moriyama, Katsuhiko; Togo, Hideo
Tetrahedron, 2012 , vol. 68, # 24 p. 4588 - 4595
100622-34-2
9-蒽硼酸
+
140-29-4
氰化苄
→
反应条件
1210-12-4
9-氰基蒽
反应条件
tert.-butylhydroperoxide; copper(l) iodide in N,N-dimethyl acetamide; water T=130°C; 20 h;
参考文献
Luo, Yan; Wen, Qiaodong; Wu, Zhiyuan; Jin, Jisong; Lu, Ping; Wang, Yanguang
Tetrahedron, 2013 , vol. 69, # 39 p. 8400 - 8404
→
反应条件
1210-12-4
9-氰基蒽
反应条件
2-(2-methoxyphenyl)-1-methyl-3-(diphenylphosphino)-1H-indole; potassium tert-butylate; triethylamine; bis(dibenzylideneacetone)-palladium(0) in dichloromethane; water; acetonitrile T=50°C; 24 h; Inert atmosphere;
参考文献
Yeung, Pui Yee; Tsang, Chun Pui; Kwong, Fuk Yee
Tetrahedron Letters, 2011 , vol. 52, # 52 p. 7038 - 7041
1564-64-3
9-溴蒽
→
反应条件
1210-12-4
9-氰基蒽
反应条件
1,8-bis(diisopropylphosphino)triptycene; potassium phosphate; palladium diacetate in N,N-dimethyl-formamide T=90°C; 24 h;
参考文献
Grossman, Olga; Gelman, Dmitri
Organic Letters, 2006 , vol. 8, # 6 p. 1189 - 1191
716-53-0
9-氯蒽
+
557-21-1
氰化锌
→
反应条件
1210-12-4
9-氰基蒽
反应条件
Pd0(tris(tert-butyl)phosphine)2; zinc in N,N-dimethyl acetamide T=80°C; 6 h;
参考文献
Littke, Adam; Soumeillant, Maxime; Kaltenbach III, Robert F.; Cherney, Robert J.; Tarby, Christine M.; Kiau, Susanne
Organic Letters, 2007 , vol. 9, # 9 p. 1711 - 1714
642-31-9
9-蒽甲醛
→
反应条件
1210-12-4
9-氰基蒽
反应条件
aluminum oxide; Oxonereg;; hydroxylamine hydrochloride in solid 0.133333 h; microwave irradiation;
参考文献
Bose, D. Subhas; Narsaiah, A. Venkat
Tetrahedron Letters, 1998 , vol. 39, # 36 p. 6533 - 6534
2476-68-8
1-(9-蒽基)甲胺
→
反应条件
1210-12-4
9-氰基蒽
反应条件
pyridine; trimethylamine-N-oxide; water; osmium(VIII) oxide in tetrahydrofuran T=20°C; 12 h;
参考文献
Gao; Herzig; Wang
Synthesis, 2001 , # 4 p. 544 - 546
1564-64-3
9-溴蒽
→
反应条件
1210-12-4
9-氰基蒽
反应条件
10 Pd/C; NAF; potassium iodide in PEG4000; water T=140°C; 3 h; Microwave irradiation;
参考文献
Chen, Gong; Weng, Jiang; Zheng, Zhanchao; Zhu, Xinhai; Cai, Yaoyao; Cai, Jiwen; Wan, Yiqian
European Journal of Organic Chemistry, 2008 , # 20 p. 3524 - 3528
22362-86-3
9-碘蒽
→
反应条件
1210-12-4
9-氰基蒽
反应条件
tetrabutylammomium bromide; copper (II) acetate monohydrate in water T=20 - 140°C; Microwave irradiation;
参考文献
Ren, Yunlai; Wang, Wei; Zhao, Shuang; Tian, Xinzhe; Wang, Jianji; Yin, Weiping; Cheng, Lin
Tetrahedron Letters, 2009 , vol. 50, # 32 p. 4595 - 4597
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