10,11-二氢二苯并[a,b]环庚烯-5-酮合成路线 （共 77 条）
反应条件
potassium phosphate; chlorobenzene; 2-dicyclohexylphosphino-1,1'-biphenyl; bis(dibenzylideneacetone)-palladium(0) in toluene T=105°C; 48 h;
参考文献
Symyx Technologies, Inc.
Patent: US6350916 B1, 2002 ;
Location in patent: Example 8 ;
反应条件
hydrogen in tetrahydrofuran T=20°C; P=760.051 Torr; 24 h;
参考文献
Zengin, Mustafa; Genc, Hayriye; Demirci, Tuna; Arslan, Mustafa; Kucukislamoglu, Mustafa
Tetrahedron Letters, 2011 , vol. 52, # 18 p. 2333 - 2335
反应条件
2-iodo benzoic acid; potassium hydrogen persulfate; water in acetonitrile
参考文献
Ojha, Lawanya R.; Kudugunti, Shashi; Maddukuri, Padma P.; Kommareddy, Amitha; Gunna, Meena R.; Dokuparthi, Praveen; Gottam, Hima B.; Botha, Kiran K.; Parapati, Divya R.; Vinod, Thottumkara K.
Synlett, 2009 , # 1 p. 117 - 121
反应条件
n-butyllithium; carbon dioxide in tetrahydrofuran; hexane T=-50 - 20°C; P=3878.71 Torr; Flow reactor;
参考文献
Kupracz, Lukas; Kirschning, Andreas
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 17 p. 3375 - 3380
反应条件
Nafion-H in benzene 0.5 h; Heating;
参考文献
Yamato, Takehiko; Hideshima, Chieko; Prakash, G. K. Surya; Olah, George A.
Journal of Organic Chemistry, 1991 , vol. 56, # 12 p. 3955 - 3957
反应条件
iodine in neat (no solvent) T=85°C; 0.25 h;
参考文献
Organic and Biomolecular Chemistry, , vol. 11, # 12 p. 1978 - 1999
反应条件
Nafion-H in various solvent(s) T=180°C; Acylation; Friedel-Crafts intramolecular acylation; 3 h;
参考文献
Olah, George A.; Mathew, Thomas; Farnia, Morteza; Prakash, G. K. Surya; Katherine; Donald
Synlett, 1999 , # 7 p. 1067 - 1068
反应条件
n-butyllithium in tetrahydrofuran; hexane 0.25 h;
参考文献
Poirier, Marc; Chen, Frank; Bernard, Charles; Wong, Yee-Shing; Wu, George G.
Organic Letters, 2001 , vol. 3, # 23 p. 3795 - 3798
反应条件
aluminum oxide; Ru(OH)x; oxygen in 1,2-dichloro-benzene T=169.85°C; P=760 Torr; 5 h;
参考文献
Organic Letters, , vol. 6, # 20 p. 3577 - 3580
反应条件
sodium hydroxide; tetracarbonylbis(μ-chloro)dirhodium(I); N-benzyl-N,N,N-triethylammonium chloride in benzene T=55°C; 4 h;
参考文献
Canadian Journal of Chemistry, , vol. 58, # 15 p. 1599 - 1601
