10,11-二氢二苯并[a,b]环庚烯-5-酮合成路线 (共 77 条)
反应条件
hydrogenchloride; water in acetic acid 0.5 h; Heating;
参考文献
Falshaw, Christopher P.; Hashi, Nur A.; Taylor, Giles A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 1837 - 1844
反应条件
hydrogenchloride; water in acetic acid 1 h; Heating;
参考文献
Falshaw, Christopher P.; Hashi, Nur A.; Taylor, Giles A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 1837 - 1844
反应条件
n-butyllithium; carbon dioxide in tetrahydrofuran; hexane T=-50°C; P=3878.71 Torr; Flow reactor;
参考文献
Advanced Synthesis and Catalysis, , vol. 355, # 17 p. 3375 - 3380
反应条件
PPA T=170 - 180°C; Heating;
参考文献
Stanescu, Michaela Dina; Dinca, Nicolae; Sisu, Eugen
Revue Roumaine de Chimie, 2006 , vol. 51, # 7-8 p. 669 - 673
反应条件
in methanol T=60°C; electrooxidation;
参考文献
Journal of the American Chemical Society, , vol. 109, # 17 p. 5066 - 5072
反应条件
1: 11.7 g / s-BuLi / tetrahydrofuran; cyclohexane / -20 - 25 °C 2: SOCl2 / CH2Cl2 / 20 °C 3: 77.4 percent / n-BuLi / hexane; tetrahydrofuran / 0.25 h View Scheme
参考文献
Organic Letters, , vol. 3, # 23 p. 3795 - 3798
反应条件
1: SOCl2 / CH2Cl2 / 20 °C 2: 77.4 percent / n-BuLi / hexane; tetrahydrofuran / 0.25 h View Scheme
参考文献
Organic Letters, , vol. 3, # 23 p. 3795 - 3798
反应条件
iodine in neat (no solvent) T=85°C; 18 h;
参考文献
Organic and Biomolecular Chemistry, , vol. 11, # 12 p. 1978 - 1999
反应条件
T=60°C; electroreduction;
参考文献
Journal of the American Chemical Society, , vol. 109, # 17 p. 5066 - 5072
反应条件
quartz T=550 - 800°C; Inert atmospherePyrolysis;
参考文献
Revue Roumaine de Chimie, , vol. 55, # 10 p. 711 - 714