1,3-二甲基咪唑三氟甲烷磺酸盐合成路线 （共 9 条）
反应条件
1: CF3O3S(1-)*H(1+)*H3N With Amberlyst A-26 (OH- form) in water T=20°C; 2: [mmim][I] in methanol
参考文献
Alcalde, Ermitas; Dinares, Immaculada; Ibanez, Anna; Mesquida, Neus
Molecules, 2012 , vol. 17, # 4 p. 4007 - 4027
反应条件
in hexane T=0 - 25°C; 28 h;
参考文献
Ignat'ev, Nikolai V.; Barthen, Peter; Kucheryna, Andryi; Willner, Helge; Sartori, Peter
Molecules, 2012 , vol. 17, # 5 p. 5319 - 5338
反应条件
in methanol Ionic liquidsolid phase reaction;
参考文献
Dinares, Immaculada; Garcia De Miguel, Cristina; Ibanez, Anna; Mesquida, Neus; Alcalde, Ermitas
Green Chemistry, 2009 , vol. 11, # 10 p. 1507 - 1510
反应条件
n-butyllithium 1.)hexane, CH2Cl2, -78 deg C, 10-20 min; 2.) THF, -78 deg C, 1 h, room temp., 96 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Zoller, Uri
Tetrahedron, 1988 , vol. 44, # 24 p. 7413 - 7426
反应条件
n-butyllithium 1.)hexane, CH2Cl2, -78 deg C, 10-20 min; 2.) THF, -78 deg C, 1 h, room temp., 24 h; Yield given. Multistep reaction;
参考文献
Zoller, Uri
Tetrahedron, 1988 , vol. 44, # 24 p. 7413 - 7426
反应条件
n-butyllithium
1.)hexane, CH2Cl2, -78 deg C, 10-20 min; 2.) CH2Cl2, -78 deg C, 1 h, room temp., 18 h; Yield given. Multistep reaction;
参考文献
Zoller, Uri
Tetrahedron, 1988 , vol. 44, # 24 p. 7413 - 7426
反应条件
n-butyllithium
1.)hexane, CH2Cl2, -78 deg C, 10-20 min; 2.) THF, -78 deg C, 1 h, room temp., 24 h; Yield given. Multistep reaction;
参考文献
Zoller, Uri
Tetrahedron, 1988 , vol. 44, # 24 p. 7413 - 7426
反应条件
n-butyllithium
1.)hexane, CH2Cl2, -78 deg C, 10-20 min; 2.) THF, -78 deg C, 1 h, room temp., 96 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Zoller, Uri
Tetrahedron, 1988 , vol. 44, # 24 p. 7413 - 7426
反应条件
superoxide ion
T=25°C; P=742.574 Torr; Inert atmosphere;
参考文献
AlNashef, Inas M.; Hashim, Mohd A.; Mjalli, Farouq S.; Ali, Mohammad Q. Al-haj; Hayyan, Maan
Tetrahedron Letters, 2010 , vol. 51, # 15 p. 1976 - 1978
