1: With dihydrogen peroxide; sodium carbonate; trifluoroacetic anhydride in dichloromethane T=-50°C; Epoxidation; 2: With boron trifluoride diethyl etherate in dichloromethane T=11 - 13°C; Rearrangement; 0.0333333 h; Title compound not separated from byproducts;
参考文献
Angewandte Chemie - International Edition, , vol. 39, # 3 p. 569 - 573