2-(3-甲基苯基)-1,3-苯并噻唑合成路线 （共 21 条）
反应条件
1-methyl-pyrrolidin-2-one T=100°C; 1 h;
参考文献
Brembilla, A.; Roizard, D.; Lochon, P.
Synthetic Communications, 1990 , vol. 20, # 21 p. 3379 - 3384
反应条件
γ-Al2O3 T=120°C; 0.5 h;
参考文献
Ding, Mei-Fang; Chen, Chia-Pei; Lin, Shaw-Tao
Journal of the Chinese Chemical Society, 2013 , vol. 60, # 6 p. 645 - 649
反应条件
in dichloromethane T=20°C; 1 h;
参考文献
Fukuhara, Tsuyoshi; Hasegawa, Chihiro; Hara, Shoji
Synthesis, 2007 , # 10 p. 1528 - 1534
反应条件
triethyl amine hydrochloride T=180°C; 3 h;
参考文献
Ohno; Mizukoshi; Izumi; Kato; Hori
Chemical and Pharmaceutical Bulletin, 1988 , vol. 36, # 2 p. 551 - 562
反应条件
triethyl amine hydrochloride T=180°C; 3.5 h;
参考文献
Ohno; Mizukoshi; Izumi; Kato; Hori
Chemical and Pharmaceutical Bulletin, 1988 , vol. 36, # 2 p. 551 - 562
反应条件
1: 95 percent / propan-2-ol / 2 h 2: triethylamine hydrochloride / 3 h / 180 °C View Scheme
参考文献
Ohno; Izumi; Mizukoshi; Kato; Hori
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 5 p. 1780 - 1783
反应条件
1: 95 percent / propan-2-ol / 2 h 2: triethylamine hydrochloride / 3 h / 180 °C View Scheme
参考文献
Ohno; Izumi; Mizukoshi; Kato; Hori
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 5 p. 1780 - 1783
反应条件
1.1: oxalyl chloride / CH2Cl2 / 2 h / 40 °C 1.2: 82 percent / Et3N*3HF; Et3N / CH2Cl2 / 2 h / 20 °C 2.1: 94 percent / CH2Cl2 / 1 h / 20 °C View Scheme
参考文献
Fukuhara, Tsuyoshi; Hasegawa, Chihiro; Hara, Shoji
Synthesis, 2007 , # 10 p. 1528 - 1534
反应条件
1: CuCl2·2H2O; 1,10-phenanthroline; potassium carbonate; sulfur / water / 24 h / 100 °C 2: CuCl2·2H2O; 1,10-phenanthroline; potassium carbonate; sulfur / water / 24 h / 100 °C View Scheme
参考文献
Deng, Hang; Li, Zhengkai; Ke, Fang; Zhou, Xiangge
Chemistry - A European Journal, 2012 , vol. 18, # 16 p. 4840 - 4843
反应条件
1: isopentyl nitrite / tetrahydrofuran / 0.5 h / |Reflux 2: FeCl3·6H2O; dipotassium peroxodisulfate / dimethyl sulfoxide; water / 12 h / 100 °C View Scheme
参考文献
Wang, Jian; Zhang, Xiao-Zhuan; Chen, Shan-Yong; Yu, Xiao-Qi
Tetrahedron, 2014 , vol. 70, # 2 p. 245 - 250
