Arnott, David M.; Harrison, Peter J.; Henderson, Graeme B.; Sheng, Zhi-Chu; Leeper, Finian J.; Battersby, Alan R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 265 - 278
1: 101 mg / liquid ammonia / tetrahydrofuran / -78 - 17 °C
2: 81 percent / Lawesson's reagent / toluene / 1.5 h / Heating
3: 20 mg / sodium hydride, methyl iodide, water / tetrahydrofuran / 1 h / 50 °C
View Scheme
参考文献
Arnott, David M.; Harrison, Peter J.; Henderson, Graeme B.; Sheng, Zhi-Chu; Leeper, Finian J.; Battersby, Alan R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 265 - 278
1: 101 mg / liquid ammonia / tetrahydrofuran / -78 - 17 °C
2: 81 percent / Lawesson's reagent / toluene / 1.5 h / Heating
3: sodium hydride, methyl iodide, water / tetrahydrofuran / 1 h / 50 °C
View Scheme
参考文献
Arnott, David M.; Harrison, Peter J.; Henderson, Graeme B.; Sheng, Zhi-Chu; Leeper, Finian J.; Battersby, Alan R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 265 - 278
Arnott, David M.; Harrison, Peter J.; Henderson, Graeme B.; Sheng, Zhi-Chu; Leeper, Finian J.; Battersby, Alan R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 265 - 278
Multi-step reaction with 2 steps 1: 2M potassium hydroxid / H2O / 0.75 h / 18 °C2: thionyl chloride / benzene / 0.5 h / 60 °C
参考文献
Arnott, David M.; Harrison, Peter J.; Henderson, Graeme B.; Sheng, Zhi-Chu; Leeper, Finian J.; Battersby, Alan R. Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 265 - 278
Arnott, David M.; Harrison, Peter J.; Henderson, Graeme B.; Sheng, Zhi-Chu; Leeper, Finian J.; Battersby, Alan R. Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 265 - 278
