1,3-二(吡啶-2-基)硫脲合成路线 （共 13 条）
反应条件
higher-melting form;
参考文献
Camps
Archiv der Pharmazie (Weinheim, Germany), 1902 , vol. 240, p. 358
反应条件
sodium hydroxide; Neutral lead acetate
参考文献
Feist
Archiv der Pharmazie (Weinheim, Germany), 1934 , vol. 272, p. 100,106
反应条件
triethylamine
48 h; Reflux;
参考文献
El-Ayaan, Usama
Journal of Molecular Structure, 2011 , vol. 998, # 1-3 p. 11 - 19
反应条件
in tetrahydrofuran
5 h; Heating;
参考文献
Katritzky, Alan R.; Witek, Rachel M.; Rodriguez-Garcia, Valerie; Mohapatra, Prabhu P.; Rogers, James W.; Cusido, Janet; Abdel-Fattah, Ashraf A. A.; Steel, Peter J.
Journal of Organic Chemistry, 2005 , vol. 70, # 20 p. 7866 - 7881
反应条件
in ethanol
Substitution; 4.5 h; Heating;
参考文献
Mohanta, Pramod K.; Dhar, Sanchita; Samal; Ila; Junjappa
Tetrahedron, 2000 , vol. 56, # 4 p. 629 - 637
反应条件
in ethanol
Substitution; 6 h; Heating;
参考文献
Mohanta, Pramod K.; Dhar, Sanchita; Samal; Ila; Junjappa
Tetrahedron, 2000 , vol. 56, # 4 p. 629 - 637
反应条件
sodium hydroxide in ethanol
36 h; Heating;
参考文献
Sudha, L. V.; Sathyanarayana, D. N.; Bharati, S. Narasimha
Magnetic Resonance in Chemistry, 1987 , vol. 25, p. 474 - 479
参考文献
Toptschiew
Archiv der Pharmazie (Weinheim, Germany), 1934 , vol. 272, p. 775,778
Zhurnal Obshchei Khimii, 1934 , vol. 4, p. 400,402
Full Text Show Details
Am. Cyanamid Co.
Patent: US2367569 , 1942 ;
反应条件
1: NaNH2; xylene / 140 - 150 °C
2: diethyl ether
View Scheme
参考文献
Feist
Archiv der Pharmazie (Weinheim, Germany), 1934 , vol. 272, p. 100,106
反应条件
sodium hydroxide; chloroform
higher-melting form;
参考文献
Schmid; Becker
Monatshefte fuer Chemie, 1925 , vol. 46, p. 676
