4-(2-苯基乙基)苯甲醛合成路线 （共 14 条）
反应条件
1.1: lithium hydroxide hydrate / isopropyl alcohol / 0.33 h 1.2: 16 h / Reflux 2.1: palladium 10 on activated carbon; hydrogen / toluene / 48 h / 62059.4 Torr / Autoclave 3.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere 3.2: 16 h / -78 - 20 °C / Inert atmosphere View Scheme
参考文献
Scherer, Alexander; Hampel, Frank; Gray, Murray R.; Stryker, Jeffrey M.; Tykwinski, Rik R.
Journal of Physical Organic Chemistry, 2012 , vol. 25, # 7 p. 597 - 606
反应条件
1.1: palladium 10 on activated carbon; hydrogen / toluene / 48 h / 62059.4 Torr / Autoclave 2.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere 2.2: 16 h / -78 - 20 °C / Inert atmosphere View Scheme
参考文献
Scherer, Alexander; Hampel, Frank; Gray, Murray R.; Stryker, Jeffrey M.; Tykwinski, Rik R.
Journal of Physical Organic Chemistry, 2012 , vol. 25, # 7 p. 597 - 606
反应条件
hydrogen fluoride; SbF5 T=0°C; P=15200 Torr; 2 h; composition of monoaldehyde and dialdehyde depending on the molar ratio of SbF5/dibenzyl; other substrates;
参考文献
Tanaka, Mutsuo; Fujiwara, Masahiro; Ando, Hisanori; Souma, Yoshie
Journal of Organic Chemistry, 1993 , vol. 58, # 11 p. 3213 - 3215
反应条件
hydrogen fluoride; SbF5 T=0°C; P=15200 Torr; other reagents HF-TaF5, HF-BF3, HF-NbF5, CF3SO3H-SbF5-HF; Product distributionMechanism;
参考文献
Tanaka, Mutsuo; Fujiwara, Masahiro; Xu, Qiang; Ando, Hisanori; Raeker, Todd J.
Journal of Organic Chemistry, 1998 , vol. 63, # 13 p. 4408 - 4412
