反应条件
in tetrahydrofuran
refluxing Fe-complex with Pt-complex in THF for 50 min, under N2, cooling to 22°C; evapn. of solvent, dissolution of red solid in a minimum amount of hexane, chromy. on silica gel, elution with hexane yields two yellow fractions (Fe(CO)4(PPh3) and Fe(CO)3(PPh3)2), further elution with hexane gives complex, solvent evapn., elem. anal.;
参考文献
Mirkin, Chad A.; Geoffroy, Gregory L.; Macklin, Phillip D.; Rheingold, Arnold L.
Inorganica Chimica Acta, 1990 , vol. 170, p. 11 - 16
