[[(3,5-二甲基-1H-吡咯-2-基)(3,5-二甲基-2H-吡咯-2-亚基)甲基]甲烷](二氟硼烷)合成路线 （共 7 条）
反应条件
1: 2,4-dimethyl pyrrole; acetyl chloride in dichloromethane 1.5 h; Inert atmosphereReflux; 2: With triethylamine in dichloromethane 0.25 h; Inert atmosphere; 3: boron trifluoride diethyl etherate in dichloromethane 18 h; Inert atmosphere;
参考文献
Findlay, Neil J.; Orofino-Pena, Clara; Bruckbauer, Jochen; Elmasly, Saadeldin E. T.; Arumugam, Sasikumar; Inigo, Anto R.; Kanibolotsky, Alexander L.; Martin, Robert W.; Skabara, Peter J.
Journal of Materials Chemistry C, 2013 , vol. 1, # 11 p. 2249 - 2256
反应条件
1: With triethylamine in dichloromethane T=20°C; 0.166667 h; 2: With boron trifluoride diethyl etherate in dichloromethane T=20°C; 1 h;
参考文献
Nepomnyashchii, Alexander B.; Broering, Martin; Ahrens, Johannes; Bard, Allen J.
Journal of the American Chemical Society, 2011 , vol. 133, # 22 p. 8633 - 8645
反应条件
1: dichloromethane 2: triethylamine / dichloromethane View Scheme
参考文献
Zhou, Lian; Zhu, Cheng-Cheng; Xue, Yun-Shan; He, Wei-Jiang; Du, Hong-Bin; You, Xiao-Zeng; Li, Yi-Zhi
Inorganic Chemistry Communications, 2013 , vol. 35, p. 355 - 359
反应条件
boron trifluoride diethyl etherate; triethylamine in dichloromethane
参考文献
Lin, Hsin-Yu; Huang, Wei-Ching; Chen, Yung-Chung; Chou, Hsien-Hsin; Hsu, Chih-Yu; Lin, Jiann T.; Lin, Hao-Wu
Chemical Communications, 2012 , vol. 48, # 71 p. 8913 - 8915
反应条件
triethylamine in dichloromethane
参考文献
Zhou, Lian; Zhu, Cheng-Cheng; Xue, Yun-Shan; He, Wei-Jiang; Du, Hong-Bin; You, Xiao-Zeng; Li, Yi-Zhi
Inorganic Chemistry Communications, 2013 , vol. 35, p. 355 - 359
反应条件
in chloroform-d1 detected by NMR;
参考文献
Hudnall, Todd W.; Gabbai, Francois P.
Chemical Communications, 2008 , # 38 p. 4596 - 4597
参考文献
Hendricks, J. Adam; Keliher, Edmund J.; Wan, Dongpeng; Hilderbrand, Scott A.; Weissleder, Ralph; Mazitschek, Ralph
Angewandte Chemie - International Edition, 2012 , vol. 51, # 19 p. 4603 - 4606
