(5R)-3,4,5,6-四氢-5-苯基-4(H)-1,4-恶嗪-2-酮合成路线 (共 6 条)
反应条件
N-ethyl-N,N-diisopropylamine in acetonitrile 18 h; Ambient temperature;
参考文献
Dellaria, Joseph F.; Santarsiero, Bernard D.
Journal of Organic Chemistry, 1989 , vol. 54, # 16 p. 3916 - 3926
反应条件
hydrogen; palladium on activated charcoal in ethyl acetate P=760 Torr; 3 h; Ambient temperature; Yield given;
参考文献
Journal of Organic Chemistry, , vol. 61, # 6 p. 2044 - 2050
反应条件
1: 91 percent 2: 72 percent / selenium dioxide / dioxane / 2 h / Heating 3: hydrogen / 10percent Pd-C / ethyl acetate / 3 h / 760 Torr / Ambient temperature View Scheme
参考文献
Journal of Organic Chemistry, , vol. 61, # 6 p. 2044 - 2050
反应条件
1: 72 percent / selenium dioxide / dioxane / 2 h / Heating 2: hydrogen / 10percent Pd-C / ethyl acetate / 3 h / 760 Torr / Ambient temperature View Scheme
参考文献
Journal of Organic Chemistry, , vol. 61, # 6 p. 2044 - 2050
反应条件
N-ethyl-N,N-diisopropylamine in dichloromethane T=0°C; 0.5 h;
参考文献
Dellaria, Joseph F.; Santarsiero, Bernard D.
Journal of Organic Chemistry, 1989 , vol. 54, # 16 p. 3916 - 3926
反应条件
triethylamine in ethyl acetate 6 h; Ambient temperature;
参考文献
Dellaria, Joseph F.; Santarsiero, Bernard D.
Journal of Organic Chemistry, 1989 , vol. 54, # 16 p. 3916 - 3926