三羰基-1,3,5-三甲基苯铬合成路线 (共 24 条)
参考文献
Journal of the Chemical Society, , p. 3475 - 3479
反应条件
in tetrahydrofuran addn. of equimolar amount of cyclopropene to soln. of K salt in THF under N2;; evapn. to dryness; addn. of toluene; filtration; concn.; chromy. (silica, toluene: isolation of Cr arenes, ether: isolation of Cr carbene);;
参考文献
Schubert, Juergen; Mock, Stefan; Schubert, Ulrich
Chemische Berichte, 1993 , vol. 126, # 3 p. 657 - 664
反应条件
Kinetics; byproducts: CO;
参考文献
Zeitschrift fuer Naturforschung, , vol. 22b, p. 260 - 263
反应条件
in toluene dropwise addn. of a soln. of Cr(CO)3(mes) to an ethylendiamine extract of a melt of nominal composition K4Sn9; cryptand then added as solid;; filtering twice of soln., left at 25°C, needles after 48h, elem. anal.;
参考文献
Eichhorn, Bryan W.; Haushalter, Robert C.; Pennington, William T.
Journal of the American Chemical Society, 1988 , vol. 110, p. 8704 - 8706