(2E)-2-(4-甲基戊-3-烯亚基)琥珀醛合成路线 （共 4 条）
反应条件
pyridine; Dess-Martin periodane in dichloromethane T=20°C; Dess-Martin oxidation; 2 h;
参考文献
Shimizu, Nobuhiro; Mori, Naoki; Kuwahara, Yasumasa
Bioscience, biotechnology, and biochemistry, 2003 , vol. 67, # 8 p. 1732 - 1736
反应条件
pyridine; Dess-Martin periodane in dichloromethane T=20°C; Dess-Martin oxidation; 2 h;
参考文献
Shimizu, Nobuhiro; Mori, Naoki; Kuwahara, Yasumasa
Bioscience, biotechnology, and biochemistry, 2003 , vol. 67, # 8 p. 1732 - 1736
反应条件
1: 65 percent / benzene / Heating 2: 1.) n-BuLi / 1.) ether, hexane, -5 deg C, 0.5 h, 2.) ether, RT, 0.5 h 3: 88.7 percent / TsOH / methanol / 0.5 h / Ambient temperature 4: 4 percent / PDC / CH2Cl2 / 1.5 h View Scheme
参考文献
Leal, Walter Soares; Kuwahara, Yasumasa; Suzuki, Takahisa
Agricultural and Biological Chemistry, 1989 , vol. 53, # 3 p. 875 - 878
参考文献
Shimizu, Nobuhiro; Mori, Naoki; Kuwahara, Yasumasa
Bioscience, Biotechnology and Biochemistry, 2001 , vol. 65, # 8 p. 1724 - 1728
