反应条件
1: 80 percent / CAN / H2O; acetonitrile / 0.5 h / 0 °C 2: 80 percent / K2CO3 / dioxane; H2O / 0.17 h / Ambient temperature 3: 1.) (CF3CO)2O, sym-collidine, 2.) K2CO3, NaBH4 / 1.) MeCN, 0 deg C, 5 min, 2.) H2O, 0 deg C to room temperature, 15 min 4: 80 percent / H2 / Pd(OH)2/C / methanol / 0.25 h View Scheme
参考文献
Bravo, Pierfrancesco; Capelli, Silvia; Crucianelli, Marcello; Guidetti, Maurizia; Markovsky, Andrey L.; Meille, Stefano V.; Soloshonok, Vadim A.; Sorochinsky, Alexander E.; Viani, Fiorenza; Zanda, Matteo
Tetrahedron, 1999 , vol. 55, # 10 p. 3025 - 3040
